added to the emulsion up to proportions of 1:3 for use
in slurry seal coats. Because emulsions contain water,
they have certain disadvantages. During freezing
weather the emulsions can freeze, and the components
can separate. Also, emulsions are difficult to store for
extended periods because they tend to break even in
unopened drums. When emulsions are shipped, the
water in the mixture takes up valuable space, which
could be used to transport hard-to-obtain materials.
FIELD IDENTIFICATION OF BITUMENS
A fairly accurate identification of bituminous
materials is necessary to make decisions regarding types
and methods of construction, types and quantities of
equipment, and applicable safety regulations. Field tests
must be performed to identify a bituminous material as
asphalt cement, asphalt cutback asphalt emulsion, road
tar, or road-tar cutback and to field-identify the grade.
Field identification of bitumens is summarized in
figure 13-29.
Test for Solubility
The first procedure in the identification of an
unknown bituminous material is to determine whether
it is an asphalt, an emulsion, or a tar. Bituminous
materials may be differentiated by a volubility test. To
perform the test, you simply dissolve an unknown
sample (a few drops, if liquid, or enough to cover the
head of a nail, if solid) in any petroleum distillate.
Kerosene, gasoline, diesel oil, or jet fuel is suitable for
this test. One or more of these distillates is usually
available to the EA in the field Since asphalt is derived
from petroleum, it will dissolve in the petroleum
distillate. If the material is an emulsion, it can be
detected by the appearance of small black globules, or
beads, which fall to the bottom of the container. Road
tar will not dissolve. If the sample is an asphalt, the
sample-distillate mix will be a dark, uniform liquid If
it is a road tar, the sample will be a dark, stringy,
undissolved mass in the distillate. You can make a check
by spotting a piece of paper or cloth with the mix. If no
stain results, the material is a tar; however, if a brown to
black stain appears, then it is asphalt. The volubility test
provides a positive method of identification.
Tests for Asphalt Cement
When the volubility test determines that the
bituminous material is an asphalt you should then
perform a pour test to distinguish whether the asphalt
material is asphalt cement or asphalt cutback. In this test
you place a small sample of asphalt into a container and
attempt to pour it at mom temperature (77°F). Since
asphalt cement is a solid at room temperature, it will not
pour. Even the highest penetration grade (200 to 300)
will not pour or immediately deform. The thickest
asphalt cutback, however, will start to pour in
13 seconds at a temperature of 77°F.
The various grades of asphalt cement are
distinguished by their hardness, as measured by a field
penetration test. For purposes of field identification,
the consistency of asphalt cement maybe approximated
at room temperature as hard (penetration 40-85),
medium (penetration 85- 150), and soft (penetration
150-300. These limitations are flexible, as complete
accuracy is not essential. You can make an
approximation of the hardness while in the field by
attempting to push a sharpened pencil or nail into the
asphalt at 77°F with a firm pressure of approximately
10 pounds. When the pencil point penetrates with
difficulty or breaks, the asphalt cement is hard. When it
penetrates slowly with little difficulty, the asphalt
cement is medium. If the pencil penetrates easily, the
asphalt cement is a high penetration or soft grade.
Tests for Asphalt Cutbacks
In addition to distinguishing asphalt cement from
asphalt cutback as discussed above, the pour test will
identify the viscosity grade of the cutback at a room
temperature of 77°F. After the pour test, the approximate
viscosity grade of the cutback is known, but the actual
type (RC, MC, SC) is not. Asphalt cement is cut back
with a petroleum distillate to make it more fluid. If the
material does not pour, it is an asphalt cement. If it pours,
it is a cutback or emulsion. It has been found that the
cutbacks of a given viscosity grade will pour like the
following substances:
3
0-
7
0-
250-
800-
30 0 0 -
A smear
Water
Light syrup
syrup
Molasses
Barely deform
test is used to distinguish an RC cutback
from an MC or SC cutback. The test is based on the fact
that RCs are cut back with a highly volatile material
(naphtha or gasoline) that evaporates rapidly. To
perform the test, you simply apply a thin smear of the
material on a nonabsorbent surface, such as a piece of
13-41